Sweetening agents including Honey
2.8.1 – SUGAR
PLANTATION WHITE SUGAR (commonly known as sugar) means the crystallized product obtained from sugarcane or sugar beet. It shall be free from dirt, filth, iron filings, and added colouring matter. Extraneous matter shall not exceed 0.1 per cent by weight. It shall also conform to the following standards, namely: —
Sr. | Parameters | Limit |
(a) | Moisture (when heated at 105 degree ± 1°C for 3 hours) | Not more than 0.5 % by weight |
(b) | Sucrose | Not less than 98 % by weight. |
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
REFINED SUGAR means the white crystallised sugar obtained by refining of plantation white sugar. It shall be free from dirt, filth, iron filings and added colouring matter. Extraneous matter shall not exceed 0.1 per cent by weight. It shall also conform to the following standards, namely: —
Sr. | Parameters | Limit |
(a) | Moisture (when heated at 105 degree ± 1°C for 3 hours) | Not more than 0.5 % by weight |
(b) | Sucrose | Not less than 99.5 % by weight. |
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
KHANDSARI SUGAR obtained from sugarcane juice by open pan process may be of two varieties, namely:
It may be crystalline or in powder form. It shall be free from dirt, filth, iron filings and added colouring matter. Extraneous matter shall not exceed 0.25 per cent by weight. It may contain sodium bicarbonate (food grade). It shall also conform to the following standards, namely: —
Sr. | Parameters | Limit | |
Khandsari Sugar (Sulphur Sugar) | Khandsari Sugar (Desi) | ||
(a) | Moisture (when heated at 105 degree ± 1°C for 3 hours) | Not more than 1.5 % by weight | Not more than 1.5 % by weight |
(b) | acid | Not more than 0.5 % by weight | Not more than 0.7 % by weight |
(c) | Sucrose | Not less than 96.5 % by weight. | Not less than 93.0 % by weight |
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
NOTE: – Khandsari sugar can be distinguished from plantation white sugar on the following characteristics, namely:
Sr. | Parameters | Limit | |
Khandsari Sugar (Sulphur Sugar) | Khandsari Sugar (Desi) | ||
(a) | Conductivity (106 mho/cm2) | 100-300 in 5% solution at 30oC | Not more than 100 in 5% solution at 30oC |
(b) | Calcium oxide (mg/100gms) | Not more than 100 | Not more than 50 |
BURA SUGAR means the fine grain size product made out of any kind of sugar. It shall be free from dirt, filth, iron filing and added colouring matter. Extraneous matter shall not exceed 0.1 per cent by weight. It shall also conform to the following standards, namely: —
Sr. | Parameters | Limit |
(a) | Sucrose Ash insoluble in dilute hydrochloric | Not less than 90.0 % by weight |
(b) | acid | Not more than 0.7 % by weight |
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
CUBE SUGAR means the sugar in the form of cube or cuboid blocks manufactured from refined crystallised sugar. It shall be white in colour, free from dirt and other extraneous contamination. It shall conform to the following standards: —
Sr. | Parameters | Limit |
(a) | Sucrose | Not less than 99.7 % by weight |
(b) | Moisture | Not more than 0.25 % by weight |
(c) | Total ash | Not more than 0.03 % by weight |
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
ICING SUGAR means the sugar manufactured by pulverizing refined sugar or vacuum pan (plantation white) sugar with or without edible starch. Edible starch, if added, shall be uniformly extended in the sugar. It shall be in form of white powder, free from dust, or any other extraneous matter.
Sr. | Parameters | Limit |
(a) | Total starch and sucrose (moisture free) | Not less than 99.0 % by weight |
(b) | Moisture | Not more than 0.80 % by weight |
(c) | Starch | Not more than 4.0 % by weight on dry basis |
2.8.2 – MISRI
MISRI means the product made in the form of candy obtained from any kind of sugar or palmyrah juice. It shall be free from dirt filth, iron filings and added colouring matter. Extraneous matter shall not exceed 0.1 per cent by weight. It shall also conform to the following standards, namely: —
Sr. | Parameters | Limit |
(a) | Total ash | Not less than 0.4 % by weight |
(b) | Total Sugar (Called, known or expressed as Sucrose) | Not more than 98.0 % by weight |
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
2.8.3 – Honey and it’s by products
Honey
Sr. | Parameters | Limit |
1. | Specific gravity at 27° C, Min. | 1.35 |
2. | Moisture, per cent. by mass, Max. | 20 |
3. | Total reducing sugars, per cent. by mass, Min. | 65 |
Carvia callosa and Honeydew honey, per cent. by mass, Min. | 60 | |
Blends of Honeydew honey with blossom honey, per cent. by mass, Min. | 45 | |
4. | Sucrose, per cent. by mass, Max. | 5 |
Carvia callosa and Honeydew honey, Max. | 10 | |
5. | Fructose to Glucose ratio (F/G Ratio) | 0.95-1.50 |
6. | Total Ash, per cent. by mass, Max | 0.50 |
7. | (a) Acidity expressed as formic acid per cent. by mass, Max, | 0.20 |
(b) Free Acidity milliequivalents acid/ 1000 g, Max | 50.0 | |
8. | Hydroxy Methyl Furfural (HMF) mg/kg, Max | 80.0 |
9. | Diastase activity, Schade units, Min | 3 |
10. | Water insoluble matters per cent. by mass, Max, | 0.10 |
For Pressed honey, per cent. by mass, Max. | 0.5 | |
11. | C4 Sugar, per cent. by mass, Max | 7.0 |
12. | Pollen count/g, Min | 25000 |
13. | Specific marker for Rice Syrup (SMR) | Negative |
14. | Trace marker for Rice Syrup (TMR) | Negative |
15. | Foreign oligosaccharides per cent., Max. | 0.1 |
16. | Proline, mg/kg, Min. | 180 |
17. | Electrical Conductivity: | |
(a) Honeys not listed under Honeydew, Max. | 0.8 mS/cm | |
(b) Honeys listed under Honeydew, Min. | 0.8 mS/cm | |
18. | (a) Δδ13C Max (Maximum difference between all measured δ 13C values); per mil | ± 2.1 |
(b) Δδ13C Fru – Glu (The difference in 13C/12C ratio between fructose and glucose); per mil | ± 1.0 | |
(c) Δδ13C (per cent.) Protein – Honey (The difference in 13C/12C between honey and its associated protein extract) per mil | ≥ – 1.0 |
Bees Wax
Beeswax is obtained from the honeycombs of bees (Family: Apidae e.g., Apis mellifera L) after the honey has been removed by draining or centrifuging. The combs are melted with hot water, steam or solar heat and the melted product is filtered and cast into cakes of yellow beeswax. White beeswax is obtained by bleaching the yellow beeswax with oxidizing agents, e.g., hydrogen peroxide, sulfuric acid, or sunlight.
Beeswax consists of a mixture of esters of fatty acids and fatty alcohols, hydrocarbons and free fatty acids; minor amounts of free fatty alcohols are also present.
Description. – (a) Yellow beeswax: Yellow or light-brown solid that is somewhat brittle when cold and presents a dull, granular, non-crystalline fracture when broken; it becomes pliable at about 35°. It has a characteristic odour of honey. (b) White beeswax: White or yellowish white solid (thin layers are translucent) having a faint and characteristic odour of honey.
Requirements: When tested in accordance with method specified in JECFA for Beeswax (INS No. 901) shall conform to the following requirement:
Sr. | Parameters | Limit |
1. | Solubility | Insoluble in water; sparingly soluble in alcohol; very soluble in ether |
2. | Melting point range, °C | 62 – 65 |
3. | Acid value | 17 – 24 |
4. | Peroxide value, Max | 5 |
5. | Saponification value | 87 -104 |
6. | Carnauba wax | Absent |
7. | Ceresin, paraffins and certain other waxes | Absent |
8. | Fats, Japan wax, rosin and soap | Absent |
9. | Glycerol and other polyols, per cent. by mass, Max. | 0.5 |
10. | Lead, mg/kg, Max. | 2.0 |
11. | Ash, per cent. by mass, Max. | 0.50 |
12. | Total Volatile matter, per cent. by mass, Max. | 0.75 |
Royal Jelly
Royal jelly is the mixture of secretions from hypopharyngeal and mandibular glands of worker bees, free from any additive. It is the food of larval and adult queens. It is a raw and natural food, unprocessed except for filtration which does not undergo addition of substances. The color, taste and the chemical composition of royal jelly are determined by absorption and transformation by the bees fed with the following two types of foods during the royal jelly production time:
10-hydroxy-2-decenoic acid (HDA): HDA is the characteristic component of royal jelly.
Requirements –
Table – Chemical requirements of royal jelly
Sr. | Characteristic | Permissible limit | |
Type 1 | Type 2 | ||
1. | Moisture content per cent. by mass, Max. | 62-68.5 | |
2. | 10-HDA per cent. by mass, Min. | 1.4 | |
3. | Protein, per cent. by mass | 11-18 | |
4. | Total sugar, per cent. by mass | 7-18 | |
5. | Fructose, per cent. by mass | 2-9 | |
6. | Glucose, per cent. by mass | 2-9 | |
7. | Sucrose, per cent. by mass, Max. | 3 | NA |
8. | Erlose, per cent. by mass, Max. | 0.5 | NA |
9. | Maltose, per cent. by mass, Max. | 1.5 | NA |
10. | Maltotriose, per cent. by mass, Max. | 0.5 | NA |
11. | Total acidity, ml of 1 mol/l NaOH l/100 g | 30.0-53.0 | |
12. | Total lipid, per cent. by mass | 2-8 | |
13. | C13/C12 Isotopic ratio (δ ‰) | −29 to −20 | −29 to −14 |
2.8.4: GUR OR JAGGERY
GUR OR JAGGERY means the product obtained by boiling or processing juice extracted from palmyra palm, date palm or coconut palm. It shall be free from substances deleterious to health and shall conform to the following analytical standards, on dry weight basis: –
Sr. | Parameters | Limit |
(a) | Total sugars expressed as invert sugar | Not less than 90 % & sucrose not less than 6 |
(b) | Extraneous matter insoluble in water | Not more than 2 % |
(c) | Total ash | Not more than 6 % |
(d) | Ash insoluble in hydrochloric acid (HCl) | Not more than 0.5 % |
Gur or jaggery other than that of the liquid or semi liquid variety shall not contain more than 10% moisture.
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
Sodium bicarbonate, if used for clarification purposes, shall be of food grade quality.
CANE JAGGERY OR CANE GUR means the product obtained by boiling or processing juice pressed out of sugarcane (Saccharum officinarum). It shall be free from substances unsafe to health and shall confirm to the following analytical standards on dry weight basis: –
Sr. | Characteristics | Permissible limit |
1. | Moisture, per cent. by mass, Max | 7.0 |
2. | Sucrose, per cent. by mass, Min | 70.0 |
3. | Total Sugars, Min | 90.0 |
4. | Reducing sugars, per cent. by mass, Max | 20.0 |
5. | Sulphate ash, per cent. by mass, Max | 4.0 |
6. | Ash insoluble in dilute hydrochloric acid, per cent. by mass, Max | 0.5 |
7. | Extraneous matter and water insoluble matter, per cent. by mass, Max | 2.0 |
Sodium bicarbonate, if used for clarification purpose, shall be of food grade quality.
Food Additives
Additives permitted under these regulations shall be used. Added colour shall not be permitted.
Hygiene
The product shall be prepared and handled in accordance with the guidelines specified in Schedule 4, Part-II of the Food Safety and Standards (Licensing and Regulation of Food Businesses) Regulations, 2011 and any other guidelines as provided from time to time under the Act.
Contaminants, Toxins and Residues
The product covered in this standard shall comply with the Food Safety and Standards (Contaminants, toxins and Residues) Regulations, 2011.
2.8.5: DEXTROSE
Sr. | Characteristics | Permissible limit |
1. | Sulphated ash | Not more than 0.1 % on dry basis |
2. | Acidity | 0.5 gm. Dissolved in 50 ml. of freshly boiled and cooled water requires for neutralization not more than 0.20 ml. of N/10 sodium hydroxide to phenolphthalein indicator |
3. | Glucose | Not less than 99.0 per cent on dry basis |
When heated with potassium cupritartarate solution it shall produce a copious precipitate of cuprous oxide. It shall conform to the following standards: —
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
2.8.6: GOLDEN SYRUP
GOLDEN SYRUP means the syrup obtained by inversion of sugar. It shall be golden yellow in colour, pleasant in taste and free from any crystallization.
It shall conform to the following standards: —
Sr. | Characteristics | Permissible limit |
1. | Moisture | Not more than 25.0 per cent by weight |
2. | Total Ash | Not more than 2.5 per cent by weight |
3. | Total Sugar as invert sugar | Not less than 72.0 per cent by weight |
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
Sodium bicarbonate, if used, for clarification purposes, shall be of Food Grade Quality.
2.8.7: DRIED GLUCOSE SYRUP
DRIED GLUCOSE SYRUP means the material in the form of coarse or fine, white to creamish white powder, sweet to taste, bland in flavour and somewhat hygroscopic. It shall be free from fermentation, evidence of mould growth, dirt or other extraneous matter or added sweetening or flavouring agent.
It shall also not contain any added natural or coaltar food colour. It shall conform to the following standards: —
Sr. | Characteristics | Permissible limit |
1. | Total solid contents | Not less than 93.0 per cent by weight |
2. | Reducing sugar content | Not less than 20.0 per cent by weight |
3. | Sulfated Ash | Not more than 1.0 per cent by weight |
The product may contain food additives permitted in FSS (Food Products Standards and Food Additives) Regulation.
2.8.8: Sodium Saccharin (Food Grade)-
Sodium Saccharin is white crystals or white crystalline powder. It is odour less or having a faint odour. It is intensely sweet to taste, even in dilute solution. 1 g is soluble in 1.5 ml of water and in about 50 ml of alcohol. When tested in accordance with method specified in Indian Standard, IS 5345, it shall conform to the following standards:
Sr. | Characteristics | Permissible limit |
1. | Purity as C7H4NNaO3S, after drying at 120°C for 4 h, per cent. by mass, min | 99.0 |
2. | Moisture, per cent. by mass, Max | 15.0 |
3. | Acidity and alkalinity | To pass the test |
4. | Benzoate and salicylate | To pass the test |
5. | Readily carbonizable substances | To pass the test |
6. | Toluene sulfonamides, ppm, Max | 25.0 |
Hygiene The product shall be prepared and handled in accordance with the guidelines specified in Schedule 4, Part-II of the Food Safety and Standards (Licensing and Regulation of Food Businesses) Regulations, 2011 and any other guidelines as provided from time to time under the Act.
Contaminants, Toxins and Residues The product covered in this standard shall comply with the Food Safety and Standards (Contaminants, toxins and Residues) Regulations, 2011. The products covered in this standard shall confirm to the microbiological requirements specified in Appendix B of these regulations.
Packaging and Labelling The product shall comply with the packaging and labelling requirements as specified in the Food Safety and Standards (Packaging and Labelling) Regulations, 2011.
2.8.9: ASPARTYL PHENYL ALANINE METHYL ESTER (ASPERTAME)
The loss on drying of the material at 105oC for 4 hours shall not be more than 4.3 per cent of its weight. The sulphate ash shall not be more than 0.2 per cent. It shall not contain more than 1 per cent of diketo-piper-azine.
2.8.10: Acesulfame Potassium
Acesulfame Potassium commonly known as Acesulfame-K, having empirical formula C4H4KNO4S, molecular weight as 201.24 shall be the material which is odourless, white crystalline powder having intensely sweet taste and is very slightly soluble in ethanol but freely soluble in water. It shall contain not less than 99 per cent and not more than 101 per cent of Acesulfame-K on dried basis. It shall not contain more than 3 ppm. Flouride. Heavy metals content shall not be more than 10 ppm. The loss on drying of material at 105 degree centigrade for two hours shall not be more than 1 percent of its weight.
2.8.11: Sucralose
Chemical name –
1, 6-Dichloro-1, 6-Dideoxy-β-D-Fructofuranosyl-4-Chloro-4-Deoxy-aD-galactopyranoside;
Synonyms –
4, 1 ‘6’-Trichlorogalactosucrose; INS 955
Chemical formula –
C12H19CI3O8 Molecular
weight- 397.64
It shall be white to off-white, odourless, crystalline powder, having a sweet taste. It shall be freely soluble in water, in methanol and in alcohol and slightly soluble in ethyl acetate. It shall contain not less than 98.0% and not more than 102.0% of C12H19CI3O8 calculated on anhydrous basis. It shall not contain more than 3PPM of Arsenic (as AS) and 10PPM or heavy metals (as Pb). It shall not contain more than 0.1% of methanol. Residue on ignition shall not be more than 0.7% and water not more than 0.2%.
2.8.12: Calcium Saccharin (Food Grade)
Calcium Saccharin is white crystals or white crystalline powder. It shall be odourless or having a faint odour and an intensely sweet taste even in dilute solution. One gram is soluble in 1.5 ml of water. When tested in accordance with method specified in Indian Standard, IS 5345, it shall conform to the following standards:
Sr. | Characteristics | Permissible limit |
1. | Purity as C14H8CaN2O6S2, on dry basis, per cent. by mass, Min | 99.0 |
2. | Moisture, per cent. by mass, Max | 15.0 |
3. | Benzoate and salicylate | To pass the test |
4. | Readily carbonizable substances | To pass the test |
5. | Toluene sulfonamides, ppm, Max | 25.0 |
Hygiene
The product shall be prepared and handled in accordance with the guidelines specified in Schedule 4, Part-II of the Food Safety and Standards (Licensing and Regulation of Food Businesses) Regulations, 2011 and any other guidelines as provided from time to time under the Act.
Contaminants, Toxins and Residues
The product covered in this standard shall comply with the Food Safety and Standards (Contaminants, toxins and Residues) Regulations, 2011. The products covered in this standard shall confirm to the microbiological requirements specified in Appendix B of these regulations.
Packaging and Labelling
The product shall comply with the packaging and labelling requirements specified in the Food Safety and Standards (Packaging and Labelling) Regulations, 2011.
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